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Old 05-19-2012, 10:35 PM
popi popi is offline
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Smile 8 minute rt morph cook to diamorph via...

Swip has the 2001 PDF were morphine hc is converted to the all famous diamorphine which is for the uneducated 'heroin'in 8minutes! .Untill the year 2000 it took 8'hr to 12hr ,185 degree temp with aa,'acetic anhydryde to bond morph to diamorph.Mixed with 4-DMAP at room temperature with small ammount of aa it's done in 8 minutes!.Amazing progress if you have aa' can it bee worked around with out the aa, due to it's unavailability? :Here's the PDF Title = (4-Dimethylaminopyridine as a catalyst in heroin synthesis)
S. Klemenc*
Forensic Science Institute, Ministry of the Interior, Vodovodna 95, 1000 Ljubljana, Slovenia
Received 20 March 2002; received in revised form 1 June 2002; accepted 16 July 2002

Last edited by popi; 08-24-2012 at 12:42 AM. Reason: added the pdf,for proof,sorry for delay,thanks
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Old 05-20-2012, 08:38 PM
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Default Re: 8 minute rt morph cook to diamorph via...

AA is simple enough to make.
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Old 05-21-2012, 01:30 AM
Hydroponichronic Hydroponichronic is offline
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Default Re: 8 minute rt morph cook to diamorph via...

Why use AA? Acetyl Chloride would be almost instantaneous. One would just just need some pyridine or something in the rxn to soak up the HCl.
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