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Amphetamine Synthesis: Hydrogen Iodide Ephadrine Reduction

by HeXeN


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Hydrogen iodide Reduction of Ephadrine HCL

Apparatus:

Reaction vessle 2000 mls (2lt)

Slant joint for normal distilation

400 mm ALLIHN type condenser (any water cooled condenser wich can be used for refluxing)

1000 ml graduated beaker

1000 ml pyrex baking dish

bunsen burner / heat source

morter and pestle

scientific filter paper

(here i will list products needed to extract pure elements ( this is added only for people who don't have access to element form Crystal iodine and Red phosphorus))

Chemicals:-

PH up + down kit

100 grams Ephadrine HCL (sudafed or some other brand of anti cold over the counter medication containing more then 50 mgs of ephadrine hcl in each tablet / capsuel)

150 grams RP Red Phosphorus ( approxx. 500 box's worth of SAFETY MATCH Striker pads)

150 grams crytsal iodine (I2) (five bottles of iodine liquid containing atleast 40 % iodine or more PER BOTTLE)

dH-O-H (h-o-h) H20 200 ml(distilled water)

you say ( H-O-H ) ??? thats not water.. yes it is, and i am not going to give a lecture about permanent dipole, and how oxygen holds electrons more strongly then hydrogen does and so the oxygen atom accumulates a negative electrical charge, while the hydrogens have a positive charge. so shut up.

5 liters 99% pure ethanol, (methylated spirits)

Method:-

1. (skip this if you allready have pure Red phosphorus.)

cut the striker pads off all the boxes and put them in a large glass container.. and cover with Ethanol. i found the best way is to use a tooth brush and scrub the Red phosphorus off the striker pads buy hand... but can take MANY hours to get a few grams. Altho relatively pure, it can be quite impractical for Large cooks.

(another method) take a large plastic bucket and put the Striker pads on the bottom and completely cover with ethanol. take the lid for the bucket and cut a small hole in it, to insert a power Drill with some kind of Crafted Stirring Device. put the drill on high and mix the contents of the bucket for 30 minutes to an hour.

pour the contents of the bucket threw a Mesh gauze into the pyrex tray trapping any Paper or card board. once all the mixture is pour threw the gauze u will be left with a large amount of card board wich still holds Red phosphorus, pour Ethanol threw the card board and threw the gauze into the pyrex tray to flush out any left over RED PHOSPHORUS.

in the Pyrex tray all the Red phosphorus will start to Settle on the bottom. it is a good idea to SEDMIMENT the mixture. pouring off any Excess ethanol, then flushing that back threw the gauze with the card board in it to flush out last amounts of RP.

once you believe you have gained all the red phosphorus you can from the Striker pads, Discard them and keep the RP that is still in the ethanol..

let it sit over night, then GENTLY sediment it buy Syphening or simply Pouring off the Excess ethanol, save the sludge on the bottom and let it sit in the sun for the last amount of ethanol to Evaporate off.

this will leave you with relatively pure Red phosphorus.

(note: red posphorus is flammable and burns like all fuck if you get it on your skin wile its on fire)

2. skip this step if you have pure I2 iodine crystals

pour all the iodine liquid into a large container and add 400 mls of hydrogen peroxide and 30 mls of hydrochloric acid, put in the freezer till the tempreture is ruffly 2 degree's celcious, then pour the Solution threw a scientific filter paper. the substance left in the filter will be allmost pure I2.

3. skip this step if you allready have pure ephadrine HCL

take morter and pestle and grind all the tablets to a fine powder and Dissolve in ETHANOL - shake it up to make sure All ephadrine is Disolved, now let it stand for 2 hours and gently Sedmiment the mixture To only obtain the Ethanol... all the sludge on the bottom is USELESS and is mainly for "SLOW RELEASE" into your body, throw it away and keep the cloudy looking ethanol. pour the ethanol into the Pyrex tray and apply gentle heat to evaporate the ethanol, leaving pure ephadrine HCL, in the last stage of evaporation reduce the heat as not to burn the ephadrine.

4. set up reaction vessle with stand and clamps above the heat source / bunsen burner and add 200 mls of water, and 150 grms of iodine + 100 grams of Ephadrine HCL, then add in the red phosphorus.

5. connect condenser in refluxing position and apply heat bringing the Reaction vessle solution to a Tempreture of 80 degree's celcious.

what is happening now? its not hard to understand whats going on in your Flask, but i will tell you just incase you slept threw year 12 chemistry. with the iodine - water and red phosphorus refluxing Creating Hydrogen iodide gas wich is Reducing the ephadrine to amphetamine.

after an hour increase the tempreture to 125 degree's celcious, and allow the reaction vessle solution to Reflux for 12 hours.

after 12 hours has elapsed, turn off the heat and allow reaction vessle to cool in an ice bath, remove condenser and apply slant join and condenser in position for normal distilation and apply heat to bring the solution back to 110 degree's celcious. you will notice that a yellow-ish oily liquid is flowing from the condenser into your beaker, this is basicly amphetamine, once the flow of oil from the condenser is slowing, raise the tempreture to 125 degree's celcious to force any remaining speed over into the beaker.

once the flow has completely stopped, terminate the heat source, discard left over sludge in reaction vessle and CLEAN equiptment extremely well with Ethanol- and then again with hot water and a steralizing product.

neutralize the solution in the beaker with the PH up+down kit, it dusnt have to be perfect, but the closer to neutral the better.

once solution has been neutralized, pour it into a Clean pyrex baking dish and apply gentle heat to the bottom (DO NOT ALLOW THE TEMPRETURE TO GO BEYOND 30 DEGREE'S CELCIOUS) once it has all been evaporated off you will be left with a yellow-ish to brown coloured substance, scrape it up with a razor blade and Weigh it.

add just enough ethanol to Dissolve the substance, then add the Dryed weight of the product to the same weight in EPSUM SALTS (magnesium sulfate) so if there was 80 grams of speed when dryed, add 80 grams of empsum salts to the solution.. understand?? good.

allow the ethanol to evaporate off and u will be left with a slightly yellow Crystaline substance.

this is Street level PURE amphetamine, me and you both know its not PURE PURE, (because of the addition of epsum salts in the final crystalization stage) but the fact Remains, this shit is the Shizzznitt, and is VERY STRONG, one tenth of a gram of PURE PURE speed straight from the Crystalization Tray BEFOR the addition of magnesium sulfate is enough to give you the biggest head spin and make you feel like your the blade on a helicopter for atleast 30 minutes ( the worst 30 minz of your life) then have you cleaning your mums house and wondering about the police living in your roof for the next 2 days, so take my advice and cut it befor using it. its very high quality shit, and 99% of people have never had PURE PURE speed, because 99% of cooks realise how strong it is and never sell it straight from the crystalization tray without cutting. also .. after dissolving the product with ethanol and adding Empsum salts, it gives the product a nice Crystaline appearance normmally assosiated with Speed or methamphetamines

this Tutorial was written by hexen.

the information provided here is the result of a long time of trial and error from the original recipe passed down to me from a higher power, not everything will work perfectly for you with those exact measurements and your perticular equiptment, but a few try's will get it down to a syntax, also i gained the information on extracting the Red phosphorus from a user on totse.com! props to you whoever you are :P

i hve seen users describing amphetamine synthesis that dont Require a condenser like a "one-pot" method.

i am sorry but it dusnt work, this shit MUST be refluxed for atleast 12 hours, just boiling it in a pot dusnt work, lol but really that is a dumb idea and anyone who is stupid enough to believe it Deserves to DIE FROM A DIRTY WHAK.

if you follow half the recipe's you find on the net, u Will get a dirty, WITHOUT A DOUBT, and it just may be your last.

for people out there who don't know what a dirty is, its when you whak up something (inject something) into your viens that has impuritie's or un-wanted nasty's in it, your body goes into convulsions, as if you are trying to Spew it back up but cant.. your body starts going Really cold, and normaLLY... you die. DO NOT FOLLOW ANY ONE POT RECIPE's - or basicly any recipe's that dont follow basicly what i have just Described, except of course for different chemicals used to create Hydrogen iodide, example:-

hypophosphorus acid is commonly used and is very safe and effective in the process of creating hydrogen iodide.

i seen one Recipe that started off, dissolving MAGNESIUM in some liquid - i suggest you keep well clear of a synthesis that starts like that.

one more thing, its not completely nessesary to prepare Pre-made hydrogen iodide as a liquid, refered to hydriodic acid or HI(aq) as it is formed instantly with the addition of red phosphorus water and iodine under heat.

 
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